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PCCA PostersAtrevis Journal Articles

  • Testosterone Therapy for Late-Onset Hypogonadism: A Clinical, Biological, and Analytical Approach Using Compounded Testosterone 0.5–20% Topical Gels Pharmaceutics pcca logo Abstract
    Abstract: Testosterone is integral to men’s sexual and overall health, but there is a gradual decline in the ageing male. The topical administration of testosterone is a valuable option as a supplement (replacement) therapy to alleviate hypogonadal symptoms. The clinical efficacy of a compounded testosterone 5% topical gel was assessed retrospectively in a male patient in his seventies by evaluating the laboratory testing of the serum total testosterone and the results of a validated androgen deficiency questionnaire. After treatment, the patient’s hypogonadal symptoms improved and the serum total testosterone level achieved was considered clinically optimal. The skin permeation of the testosterone topical gel (biological testing) was evaluated in vitro using the Franz finite dose model and human cadaver skin, and it is shown that testosterone can penetrate into and through ex vivo human skin. Testosterone therapy is often prescribed for extended periods, and consequently, it is crucial to determine the beyond-use date of the compounded formulations. The analytical testing involved a valid, stability-indicating assay method for compounded testosterone 0.5% and 20% topical gels. This multidisciplinary study shows evidence supporting topically applied testosterone’s clinical efficacy and the compounded formulations’ extended stability. Personalized, topical testosterone therapy is a promising alternative in current therapeutics for hypogonadal patients.

PCCA PostersAtrevis Case Studies

Journal Article IconAtrevis Conference Abstracts

Journal Article IconAtrevis Technical Reports

Journal Article IconAtrevis Scientific Posters

PCCA PostersEctoSeal Journal Articles

  • Integrated In Vivo and In Vitro Evaluation of a Powder-to-Hydrogel, Film-Forming Polymer Complex Base with Tissue-Protective and Microbiome-Supportive Properties Gels pcca logo Abstract
    Abstract: The study aimed to perform a comprehensive in vitro and in vivo evaluation of a newly developed, patent-pending, powder-to-hydrogel, film-forming polymer complex base, which possesses tissue-protective and microbiome-supportive properties, and to compare its characteristics with poloxamer 407. The study used a combination of in vitro assays, including tissue viability and cell migration, and in vivo wound healing evaluations in male diabetic mice. Microbiome dynamics at wound sites were also analyzed. The in vitro assays demonstrated that the polymer complex base was non-cytotoxic and that it enhanced cell migration over poloxamer 407. In vivo, the polymer complex base demonstrated superior wound healing capabilities, particularly in combination with misoprostol and phenytoin, as evidenced by the reduced wound area and inflammation scores. Microbiome analysis revealed favorable shifts in bacterial populations associated with the polymer complex base-treated wounds. The polymer complex base demonstrates clinical significance in wound care, potentially offering improved healing, safety and microbiome support. Its transformative properties and efficacy in drug delivery make it a promising candidate for advanced wound care applications, particularly in chronic wound management.

PCCA PostersEctoSeal Manual

PCCA PostersEctoSeal Case Studies

PCCA PostersEctoSeal Scientific Posters

PCCA PostersEctoSeal Conference Abstracts

  • 666. In Vitro and In Vivo Evaluation of Wound Healing by Phenytoin 2% and Misoprostol 0.0024% Topical Hydrogel Journal of Investigative Dermatology pcca logo Abstract
    Abstract: Chronic wounds are a major clinical problem that leads to considerable morbidity and mortality worldwide. A newly developed wound care compounding base was incorporated phenytoin 2% and misoprostol 0.0024% for in vitro and in vivo testing. The performance of this formulation was compared to a product of reference: phenytoin 2% and misoprostol 0.0024% in poloxamer gel, commonly used in wound healing. The process of re-epithelialization in vitro was evaluated using primary human keratinocytes and the Oris™ cell migration assay kit. The cells were treated with test formulations for 24 hours and then stained with Calcein AM. The process of wound healing in vivo was evaluated using the diabetic mice wound healing model (BKS-db), including 12 male mice distributed in a control group and two test groups (topical hydrogel and poloxamer formulations). Two full-thickness excisional skin wounds were made to the back of each mouse and the test formulations were applied daily on the skin wounds for a total of 9 days. Ethics approval was obtained for this animal study. Keratinocyte migration showed a mean change of 70.62% ± 43.27 (p=6.95E-06) from control for the topical hydrogel formulation, as opposed to -29.99% ± 22.85 (p=0.0007) for the poloxamer gel formulation. Keratinocyte migration is part of the re-epithelialization process in wound healing and, therefore, the topical hydrogel formulation is likely to have greater wound healing abilities than the product of reference. The mice were successfully treated for 9 days, as shown by the digital photographs of the wound areas. The mean percentage of relative wound area was lower for the topical hydrogel formulation (49.67%), when compared to the poloxamer gel formulation (71.54%) and the control group (75.44%), which reinforces the superior wound healing abilities of the topical hydrogel formulation. The authors are affiliated with Professional Compounding Centers of America (PCCA), the manufacturer of the newly developed wound care compounding base.

PCCA PostersEllage Case Studies

  • Topical/Vaginal Treatment of Sexual Function Disorders
  • Vulvovaginal Symptoms in a Postmenopausal Woman: Case Study International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: A postmenopausal female patient was suffering from vulvovaginal symptoms such as dryness and irritation, which were affecting her relationship with her partner and her overall quality of life. The patient was instructed to apply an estriol 0.1% vaginal ointment (PCCA Ellage Anhydrous Vaginal) for a duration of three months. The safety and efficacy of the compounded treatment were evaluated using an online data collection form, which included the validated Vulvovaginal Symptom Questionnaire. Post-treatment results show that the vulvovaginal symptoms were no longer bothersome, and that the patient’s relationship was no longer affected. There were no reports of undesirable effects as a result of the compounded treatment. This case study reinforces the benefits and convenience of using topical hormone replacement therapy in postmenopausal women.

PCCA PostersEllage Technical Reports

PCCA PostersEllage Scientific Posters

Journal Article IconLipoderm Journal Articles

Journal Article IconLipoderm Case Studies

PCCA PostersLipoderm Scientific Posters

Journal Article IconAnhydrous Lipoderm Technical Reports

Journal Article Icon Lipoderm USP Monographs

Journal Article Icon Lipoderm ActiveMax Journal Articles

Journal Article Icon Lipoderm HMW Journal Articles

  • Evaluation of a Compounding Phospholipid Base for the Percutaneous Absorption Of High Molecular Weight Drugs Using the Franz Finite Dose Model Skin Research & Technology pcca logo Abstract
    Background: Permeation-enhancing compounding bases are aimed to facilitate the penetration of the active pharmaceutical ingredients (APIs) across the skin barrier.
    Objectives: The purpose of this study was to evaluate the percutaneous absorption of radiolabeled human insulin (14C-isototpe) when incorporated in a proprietary phospholipid base designed to deliver APIs with high molecular weights (HMW). The aim was not to claim the transdermal delivery of insulin with potential therapeutic applications in diabetes but, instead, to evaluate the ability of the compounding phospholipid base to deliver HMW drugs.
    Methods: The percutaneous absorption of 14C-insulin was determined using human torso skin and the Franz skin finite dose model. Two topical test formulations were prepared for in vitro evaluation: insulin 1% in phospholipid base (standard) and insulin 1% in phospholipid base HMW. The rate of percutaneous absorption (mean flux) and the distribution of 14C-insulin through the skin were evaluated for both topical test formulations. A two-way ANOVA was used to determine statistical differences.
    Results: The 14C-insulin was distributed into the stratum corneum, epidermis and dermis. Mean flux values showed a rapid penetration upon application and the maximum flux was achieved at 30 min, followed by a slow decline. Subsequently, a slower decline was observed for the topical test formulation including the phospholipid base HMW.
    Conclusion: The phospholipid base HMW facilitates the percutaneous absorption of HMW drugs across human cadaver skin and, therefore, it may potentially be a useful option for compounding pharmacists and practitioners when considering the skin for the percutaneous delivery of large drugs.

Journal Article Icon Lipoderm HMW Conference Abstracts

Journal Article IconLoxaSperse Journal Articles

  • Characterization of the Properties of Powder Excipients Commonly Used in Pharmaceutical Compounding, Particulate Science and Technology  Particulate Science and Technology pcca logo Abstract
    Abstract: Capsules are the most popular and versatile dosage form produced in pharmaceutical compounding. In the preparations of capsules, powder excipients are nonactive ingredients that can be used for the purpose of increasing bulk, enhancing flow, and improving stability of a powder formulation. Flow properties of powder excipients can impact not only the compounding procedure, but also the uniformity and quality of the final product. In this study, an FT4 Powder Rheometer was used to compare dynamic, bulk, and shear properties of the following four powder excipients: Loxoral, Loxasperse, a commercial powder excipient, and lactose monohydrate. Changes in flow energy, measured as the powders are exposed to external conditions such as air, compression, consolidation, and shear forces, were used to compare flow properties of the four excipients. Results show Loxasperse to have superior dynamic properties, indicating more efficient packing potentials. Though Loxoral did not have the most favorable flow in terms of dynamic properties, Loxoral outranked the other excipients when comparing bulk and shear properties. Taking into account processing equipment and the external environment, compounding pharmacists can reevaluate current formulas to include excipients with more favorable flow properties, resulting in more uniform and higher quality products.
  • Compounding Pearls - Wound Care: Base Selection International Journal of Pharmaceutical Compounding

Journal Article IconLoxaSperse Technical Reports

Journal Article IconLoxaSperse Case Studies

PCCA PostersLoxaSperse Scientific Posters

Journal Article IconLoxOral Journal Articles

  • Case Study: Personalized Oral Low-Dose Naltrexone Titration for Pain Management International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Naltrexone is a competitive opioid receptor antagonist indicated to treat opioid and alcohol dependence. In the U.S., naltrexone is commercially available as 50-mg tablets, and the adult dosage strength typically ranges between 50 mg once daily and 100 mg once daily. However, there is evidence to suggest that naltrexone prescribed in low doses, about 1/10th of the daily standard dosage, may be effective in managing a myriad of chronic conditions, including pain refractory to conventional pharmacological treatments. The U.S. Food and Drug Administration recently granted an orphan drug designation for low-dose naltrexone for the treatment of complex regional pain syndrome. This article provides a case study of a patient who was treated with a low dose of naltrexone for pain associated with the diagnosis of idiopathic hypereosinophilic syndrome.
  • Characterization of the Properties of Powder Excipients Commonly Used in Pharmaceutical Compounding, Particulate Science and Technology  Particulate Science and Technology pcca logo Abstract
    Abstract: Capsules are the most popular and versatile dosage form produced in pharmaceutical compounding. In the preparations of capsules, powder excipients are nonactive ingredients that can be used for the purpose of increasing bulk, enhancing flow, and improving stability of a powder formulation. Flow properties of powder excipients can impact not only the compounding procedure, but also the uniformity and quality of the final product. In this study, an FT4 Powder Rheometer was used to compare dynamic, bulk, and shear properties of the following four powder excipients: Loxoral, Loxasperse, a commercial powder excipient, and lactose monohydrate. Changes in flow energy, measured as the powders are exposed to external conditions such as air, compression, consolidation, and shear forces, were used to compare flow properties of the four excipients. Results show Loxasperse to have superior dynamic properties, indicating more efficient packing potentials. Though Loxoral did not have the most favorable flow in terms of dynamic properties, Loxoral outranked the other excipients when comparing bulk and shear properties. Taking into account processing equipment and the external environment, compounding pharmacists can reevaluate current formulas to include excipients with more favorable flow properties, resulting in more uniform and higher quality products.
  • Combination Therapy of Oral LDN and Topical Pentoxifylline, Rifampin, Clindamycin for Hidradenitis Suppurativa International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Hidradenitis Suppurativa (HS) is a chronic inflammatory skin disease that may have profound effects on the patient’s quality of life. A personalized HS combination therapy treatment was prescribed to a 54-year-old female suffering from multiple painful sores, as follows: naltrexone capsules titrated from 0.5 mg up to 4.5 mg; pentoxifylline 5%, rifampin 2%, clindamycin 1%, and glycolic acid topical cream. Clinical improvements were observed using two disease-specific outcome measures: Hurley Staging System and HS Score. The patient’s HS improved from Stage II (moderate) to Stage I (mild), and the HS score decreased from 103 points with five anatomical regions reported, to 19 points with only three regions affected. Furthermore, the before and after treatment photographs showed a visible reduction in the number of boils/skin abscesses and an overall recovery. Improvements were also observed across all domains of the patient’s self-reported quality of life (Hidradenitis Suppurativa Quality of Life Assessment). The patient did not experience any undesirable effects. Compounded medications may be customized to meet the patient’s special needs and may be adjusted throughout the course of treatment to match the patient’s individual progress. Although further studies are necessary, this personalized, combination therapy may be a key treatment option in HS.
  • Investigation of the Bioaccessibility of Progesterone (Micronized and Nonmicronized), Using an In Vitro Model of the Human Gastrointestinal System  International Journal of Applied Science and Technology pcca logo Abstract
    Abstract: The aim of this study is to evaluate the bioaccessibility of two progesterone oral formulations (micronized progesterone 100 mg SR capsules and milled progesterone 100 mg SR capsules), using an in vitro model of the human GI tract. Results show that overall bioaccessibility of micronized progesterone (21.8%) was significantly greater than that of milled progesterone (1.9%), p < 0.001. The higher total bioaccessibility could potentially be due to the smaller particle size of micronized progesterone (< 6 μm), in comparison to that of milled progesterone (approximately 92 μm). One may hypothesize that oral compounded micronized progesterone has the potential for greater bioavailability because of the significantly higher bioaccessibility of micronized progesterone in comparison to milled progesterone. Knowledge of this study’s results may be useful for practitioners when justifying the viability of using micronized progesterone over milled progesterone in the management of postmenopausal symptoms.

PCCA PostersLoxOral Case Studies

  • Case Study: Personalized Oral Low-Dose Naltrexone Titration for Pain Management International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Naltrexone is a competitive opioid receptor antagonist indicated to treat opioid and alcohol dependence. In the U.S., naltrexone is commercially available as 50-mg tablets, and the adult dosage strength typically ranges between 50 mg once daily and 100 mg once daily. However, there is evidence to suggest that naltrexone prescribed in low doses, about 1/10th of the daily standard dosage, may be effective in managing a myriad of chronic conditions, including pain refractory to conventional pharmacological treatments. The U.S. Food and Drug Administration recently granted an orphan drug designation for low-dose naltrexone for the treatment of complex regional pain syndrome. This article provides a case study of a patient who was treated with a low dose of naltrexone for pain associated with the diagnosis of idiopathic hypereosinophilic syndrome.

Journal Article IconLoxOral Technical Reports

PCCA PostersLoxOral Scientific Posters

Journal Article IconMucoLox Journal Articles

  • Budesonide 1-mg/10-mL and 2-mg/10-mL Mucolox Oral Suspensions International Journal of Pharmaceutical Compounding
  • Case Report of a Human Pappilomavirus Infection Treated with Green Tea Extract and Curcumin Vaginal Compounded Medications  International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: The human papillomaviruses are the most common sexually transmitted infections in the U.S., and the majority of these infections are cleared by the body's natural immune system without causing any harm. The high-risk human papillomavirus types, however, cause approximately 5 percent of all cancers worldwide. A prophylactic vaccine was recently introduced, but there is still no commercially available treatment that targets active infections. This case study discusses a 48-year-old female who was diagnosed as human papillomavirus positive (+) following a routine gynecological examination. Upon discussion with a compounding pharmacist, the obstetrician/gynecologist prescribed Green Tea Extract 15% Vaginal Cream and Curcumin 250 mg Vaginal Suppositories, to be applied on alternate days for a period of 3 months. After only 1 month of treatment, the gynecologic cytology report tested negative for human papillomavirus. The patient was very satisfied with the compounded medications prescribed (treatment satisfaction questionnaire) and the human papillomavirus (+) diagnosis was reported to have only little/moderate impact on the patient’s sexual life (Human Papillomavirus Impact Profile questionnaire). The successful results obtained in this case study confirm the beneficial properties of green tea extract and curcumin against the viruses, and highlight the key role of pharmaceutical compounding in current therapeutics.
  • Compounding Pearls - Wound Care: Base Selection International Journal of Pharmaceutical Compounding
  • Dexamethasone Solution and Dexamethasone in Mucolox™ for the Treatment of Oral Inflammatory Ulcerative Diseases: A Phase II Randomized Clinical Trial Journal of Oral Pathology & Medicine pcca logo Abstract
    Background: Mucolox™ is a mucosal drug delivery system that prolongs the contact time between the oral mucosa and topical corticosteroids, potentially reducing the need for multiple applications daily. This study aimed to assess the clinical efficacy and tolerability of dexamethasone 0.5 mg/5 mL solution in Mucolox™ for the management of oral inflammatory ulcerative diseases.

    Methods: Participants were randomly assigned to receive dexamethasone 0.5 mg/5 mL in Mucolox™ (Mucolox™ arm) or dexamethasone 0.5 mg/5 mL solution (standard arm) and instructed to swish/gargle for 5 min three times daily. Changes from pre- to posttreatment patient's sensitivity score (0–10 on a visual analog scale), reticulation/erythema/ulceration score, and oral health-related quality of life were evaluated at baseline and at the end of the study period.

    Results: Twenty nine patients (75% females) with a median age of 58 years (range 18–79) were enrolled and randomly allocated to the Mucolox™ or standard arm. One subject was excluded. Although statistically significant in both arms, the pre- to posttreatment sensitivity score reduction was higher in the Mucolox™ arm (6.3 vs. 4.4-point reduction). Both arms showed a decrease in the reticulation/erythema/ulceration score between the two visits (7.2 vs. 4.7 [Mucolox™ arm]; 8.0 vs. 4.8 [standard arm]; p > 0.05). Mucolox™ in dexamethasone 0.5 mg/5 mL solution was better tolerated when taste and level of comfort were considered.

    Conclusion: Both treatments were effective in the management of oral inflammatory ulcerative diseases. Dexamethasone 0.5 mg/5 mL in Mucolox™ was better tolerated and was slightly better in controlling patients' oral sensitivity. Larger studies are needed to confirm these findings in oral inflammatory ulcerative diseases patients.

  • Dexamethasone Solution and Dexamethasone In Mucolox for the Treatment of Oral Lichen Planus: a Preliminary Study Oral Surgery Oral Medicine Oral Pathology Oral Radiology pcca logo Abstract
    Objective: The objective of this single-center, open-label, randomized, phase II study was to evaluate the safety and efficacy of dexamethasone 0.1 mg/mL solution in Mucolox (arm A) compared with dexamethasone 0.1 mg/mL solution alone (arm B) for treatment of oral lichen planus (OLP).

    Study Design: Patients with clinical OLP and visual analog scale (VAS) sensitivity scores 7 or greater were randomized to arm A or B. Reticulation/erythema/ulcer (REU) scores, VAS for sensitivity and the Chronic Oral Mucosal Diseases Questionnaire (COMDQ) were completed at the baseline and the end of treatment (4 weeks). Differences were assessed by using Wilcoxon's rank-sum test.

    Results: Twenty-four patients (females n = 21; median age 64.5 years; range 45–80 years) were randomly assigned to arm A or B. Four patients were excluded. Dexamethasone with or without the addition of Mucolox was effective at reducing the REU score, but the Mucolox-containing solution was relatively more effective (6-point reduction vs 4.3-point reduction; P < .001). There was significant improvement in the total COMDQ score in both arms (mean change 1.8 [arm A] vs 2.5 [arm B]). There were no differences in compliance between the 2 study arms (P = .58).

    Conclusion: Dexamethasone 0.1 mg/mL solution in Mucolox was more effective for the management of OLP compared with dexamethasone 0.1 mg/mL solution alone. Larger studies are needed to confirm these preliminary findings.

  • Effects of Compounded Stanford Modified Oral Rinse (MucoLox) on the Survival and Migration of Oral Keratinocytes and Fibroblasts: Implications for Wound Healing International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Several oral rinses are commercially available to alleviate the symptoms of oral mucositis. Prolonged retention of active pharmaceutical ingredients in the oral cavity is a major problem. In this study, we modified the Stanford oral rinse by including a proprietary mucoadhesive polymer called MucoLox, which we hypothesized would improve active pharmaceutical ingredient mucoadhesion. Characterization of this newly compounded oral rinse showed absence of cytotoxicity in human oral keratinocyte and fibroblast cell lines. The compounded formulation significantly stimulated the migration of these two cell lines in Oris Cell Migration Assay plates, better than the reference commercial product Magic mouthwash. Based on this in vitro study, the new Stanford modified oral rinse with MucoLox is safe and may promote healing of oral mucositis.
  • Evaluation of the Safety, Cell Migration and Mucoadhesive Properties of a Mucoadhesive Polymer Blend in Human Oral Mucosa AAPS PharmSciTech pcca logo Abstract
    Abstract: The efficacy of active pharmaceutical ingredients (API) in compounded medications for oral mucosa greatly depends on the composition of the base. Here, we assessed the safety, facilitation of cell migration, and mucoadhesive properties of a newly developed mucoadhesive polymer blend (MPB) which contains pullulan, tamarindus indica polysaccharide, and sodium hyaluronate. No cell death was observed when human oral keratinocyte (HOK) and fibroblast (HOrF) cells were exposed to 1% MPB for 24 h. Epithelial cells in a 3D buccal tissue model (EpiOral) were unaffected when exposed to 50% MPB for 20 h whereas 1% Triton X-100 killed 93% cells after 4.5 h. The expressions of cytokines IL1α and IL1β and cell proliferation markers PCNA, CYCLIN A, and CYCLIN D1 in EpiOral tissue did not increase suggesting that MPB is neither an irritant nor a mitogen. Markers of apoptosis such as cleavage of CASPASES 8/9, upregulation of pro-apoptosis NOXA protein, and downregulation of anti-apoptosis XIAP protein were observed in Triton X-100-treated cells but not in cells exposed to MPB. The migration of HOK and HOrF cells was stimulated by MPB, and the expression of E-CADHERIN in the EpiOral tissues was unaffected. Moreover, MPB showed stronger mucoadhesion on the human EpiOral tissue model compared with a reference product. We conclude that MPB can safely deliver API within the oral mucosa, facilitate cell migration, and may increase drug efficacy through its strong mucoadhesive property.
  • Physical and Chemical Stability of Budesonide Mucoadhesive Oral Suspensions (MucoLox) International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Budesonide is a corticosteroid that has been shown effective in the treatment of eosinophilic esophagitis, but there are currently no commercial medicines to treat this chronic allergic/immune condition, despite its prevalence in the U.S. Therefore, pharmaceutical compounding is the alternative choice to meet the therapeutic need of eosinophilic esophagitis patients. Two budesonide mucoadhesive oral suspensions (1 mg/10 mL and 2 mg/10 mL) were developed using the compounding vehicle MucoLox, a proprietary mucoadhesive polymer blend that promotes mucosal adhesion. The physical and chemical stability of the oral suspensions was tested over a period of 182 days, at room temperature and refrigerated conditions, in order to determine the corresponding beyond-use date. The physical characterization consisted in observing all samples for color/appearance and odor, and testing for pH and density, whereas the chemical characterization consisted in ultra-performance liquid chromatography assay testing. Both oral suspensions were proven physically and chemically stable, and the ultra-performance liquid chromatography method was proven stability indicating. As a result, the beyond-use date of the budesonide 1-mg/10-mL and 2-mg/10-mL mucoadhesive oral suspensions (MucoLox), in amber plastic bottles, is six months at both room temperature and refrigerated conditions.

Journal Article IconMucoLox Technical Reports

Journal Article IconMucoLox Case Studies

  • Case Report of a Human Pappilomavirus Infection Treated with Green Tea Extract and Curcumin Vaginal Compounded Medications  International Journal of Pharmaceutical Compounding Abstract
    Abstract: The human papillomaviruses are the most common sexually transmitted infections in the U.S., and the majority of these infections are cleared by the body's natural immune system without causing any harm. The high-risk human papillomavirus types, however, cause approximately 5 percent of all cancers worldwide. A prophylactic vaccine was recently introduced, but there is still no commercially available treatment that targets active infections. This case study discusses a 48-year-old female who was diagnosed as human papillomavirus positive (+) following a routine gynecological examination. Upon discussion with a compounding pharmacist, the obstetrician/gynecologist prescribed Green Tea Extract 15% Vaginal Cream and Curcumin 250 mg Vaginal Suppositories, to be applied on alternate days for a period of 3 months. After only 1 month of treatment, the gynecologic cytology report tested negative for human papillomavirus. The patient was very satisfied with the compounded medications prescribed (treatment satisfaction questionnaire) and the human papillomavirus (+) diagnosis was reported to have only little/moderate impact on the patient’s sexual life (Human Papillomavirus Impact Profile questionnaire). The successful results obtained in this case study confirm the beneficial properties of green tea extract and curcumin against the viruses, and highlight the key role of pharmaceutical compounding in current therapeutics.
  • Palliative Care: Chemoradiation Therapy-Induced Oral Mucositis

PCCA PostersMucoLox Scientific Posters

Journal Article Icon Mucolox USP Monographs

Journal Article IconPracaSil-Plus Journal Articles

  • A Topical Naltrexone Formulation for Surgical Wound Healing: A Case Report Journal of Cosmetic Dermatology pcca logo Abstract
    Background: In current guidelines, there is no specific therapeutic recommendation for promoting surgical wound healing. Proper postsurgical wound care regimen can speed up wound healing and prevent abnormal scarring.

    Aims: The purpose of this case study was to evaluate the effectiveness of a compounded topical formulation containing naltrexone in managing surgical wound in a patient after Mohs micrographic surgery (MMS).

    Patients/Methods: A patient started to apply the topical naltrexone formulation two days after the MMS on his hand. Images of the wound and a Patient Scar Assessment Questionnaire (PSAQ) were used to evaluate the clinical outcomes.

    Results: The wound completely healed, and the hand function was fully recovered following application of the formulation for 2 weeks. No abnormal scarring was formed, and the scar was only slightly noticeable after 2 months.

    Conclusion: This case study demonstrated the effectiveness of the topical naltrexone formulation in surgical wound management.
  • Case Reports on the Use of Aloe Vera, Naltrexone, and Topiramate for the Treatment of Scars International Journal of Pharmaceutical Compounding
  • Case Report: Diabetic Foot Ulcer Infection Treated With Topical Compounded Medications International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: An adult diabetic male with three toes amputated on his right foot presented with an ulcer infection on his left foot, unresponsive to conventional antifungal oral medication for over two months. The ulcerated foot wound had a large impairment on the patient’s quality of life, as determined by the Wound-QoL questionnaire. The compounding pharmarcist recommended and the physician prescribed two topical compounded medicines, which were applied twice a day, free of charge at the compounding pharmacy. The foot ulcer infection was completely resolved following 13 days of treatment, with no longer any impairment on the patient’s quality of life. This scientific case study highlights the value of pharmaceutical compounding in current therapeutics, the importance of the triad relationship, and the key role of the compounding pharmacist in diabetes care.
  • Clotrimazole 2%, Ibuprofen 2%, Metronidazole 2%, Nifedipine 0.2%, and Dexpanthenol 3% in PracaSil-Plus US Pharmacist: A Jobson Publication
  • Compounding Pearls - Wound Care: Base Selection International Journal of Pharmaceutical Compounding
  • Pitch Ointment: Applications in Scar and Wound Management  International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: There is a high incidence of household knife-related injuries requiring emergency department treatment in the U.S. The Pitch Ointment, a named formula developed by a compounding pharmacist, was used separately by two patients who suffered a knife injury in a finger and a foot. This formula combines Pinene (L-Alpha) 0.5% and Canada Balsam 5% in PracaSil-Plus, special ingredients with applications in scar and wound healing. The patients’ level of satisfaction with the Pitch Ointment was very high since all 4 treatment satisfaction domains by the Treatment Satisfaction Questionnaire for Medication (effectiveness, side effects, convenience, global satisfaction) were rated over 85. These results are consistent with the clinical improvements observed in the before and after treatment photographs. The success of these case reports is evidence to suggest that the Pitch Ointment may be recommended by compounding pharmacists as a viable treatment option in scar and wound management.

Journal Article IconPracaSil-Plus Technical Reports

Journal Article IconPracaSil-Plus Case Studies

  • A Topical Naltrexone Formulation for Surgical Wound Healing: A Case Report Journal of Cosmetic Dermatology pcca logo Abstract
    div class="card-body abstracts-container"> Background: In current guidelines, there is no specific therapeutic recommendation for promoting surgical wound healing. Proper postsurgical wound care regimen can speed up wound healing and prevent abnormal scarring.

    Aims: The purpose of this case study was to evaluate the effectiveness of a compounded topical formulation containing naltrexone in managing surgical wound in a patient after Mohs micrographic surgery (MMS).

    Patients/Methods: A patient started to apply the topical naltrexone formulation two days after the MMS on his hand. Images of the wound and a Patient Scar Assessment Questionnaire (PSAQ) were used to evaluate the clinical outcomes.

    Results: The wound completely healed, and the hand function was fully recovered following application of the formulation for 2 weeks. No abnormal scarring was formed, and the scar was only slightly noticeable after 2 months.

    Conclusion: This case study demonstrated the effectiveness of the topical naltrexone formulation in surgical wound management.
  • Case Report: Diabetic Foot Ulcer Infection Treated With Topical Compounded Medications International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: An adult diabetic male with three toes amputated on his right foot presented with an ulcer infection on his left foot, unresponsive to conventional antifungal oral medication for over two months. The ulcerated foot wound had a large impairment on the patient’s quality of life, as determined by the Wound-QoL questionnaire. The compounding pharmarcist recommended and the physician prescribed two topical compounded medicines, which were applied twice a day, free of charge at the compounding pharmacy. The foot ulcer infection was completely resolved following 13 days of treatment, with no longer any impairment on the patient’s quality of life. This scientific case study highlights the value of pharmaceutical compounding in current therapeutics, the importance of the triad relationship, and the key role of the compounding pharmacist in diabetes care.
  • Case Reports on the Use of Aloe Vera, Naltrexone, and Topiramate for the Treatment of Scars International Journal of Pharmaceutical Compounding
  • Pitch Ointment: Applications in Scar and Wound Management  International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: There is a high incidence of household knife-related injuries requiring emergency department treatment in the U.S. The Pitch Ointment, a named formula developed by a compounding pharmacist, was used separately by two patients who suffered a knife injury in a finger and a foot. This formula combines Pinene (L-Alpha) 0.5% and Canada Balsam 5% in PracaSil-Plus, special ingredients with applications in scar and wound healing. The patients’ level of satisfaction with the Pitch Ointment was very high since all 4 treatment satisfaction domains by the Treatment Satisfaction Questionnaire for Medication (effectiveness, side effects, convenience, global satisfaction) were rated over 85. These results are consistent with the clinical improvements observed in the before and after treatment photographs. The success of these case reports is evidence to suggest that the Pitch Ointment may be recommended by compounding pharmacists as a viable treatment option in scar and wound management.
  • Second-degree Skin Burn Injury Following a Domestic Incident
  • Surgical Scar Management with Topical Treatment

PCCA PostersPracaSil-Plus Scientific Posters

Journal Article IconSuspendIt Journal Articles

Journal Article IconSuspendIt Technical Reports

PCCA PostersSuspendIt Scientific Posters

Journal Article Icon SuspendIt USP Monographs

Journal Article Icon SuspendIt Conference Abstracts

Journal Article IconSuspendIt Anhydrous Journal Articles

  • Analysis of the Physical Characteristics of an Anhydrous Vehicle for Compounded Pediatric Oral Liquids Pharmaceutics pcca logo Abstract
    Abstract: The paucity of suitable drug formulations for pediatric patients generates a need for customized, compounded medications. This research study was set out to comprehensively analyze the physical properties of the new, proprietary anhydrous oral vehicle SuspendIt® Anhydrous, which was designed for compounding pediatric oral liquids. A wide range of tests was used, including sedimentation volume, viscosity, droplet size after dispersion in simulated gastric fluid, microscopic examination and content uniformity measurements to evaluate the properties of the anhydrous vehicle. The results showed that the vehicle exhibited consistent physical properties under varying conditions and maintained stability over time. This can be attributed to the unique blend of excipients in its formulation, which not only maintain its viscosity but also confer thixotropic behavior. The unique combination of viscous, thixotropic and self-emulsifying properties allows for rapid redispersibility, sedimentation stability, accurate dosing, potential drug solubility, dispersion and promotion of enhanced gastrointestinal distribution and absorption. Furthermore, the vehicle demonstrated long-term sedimentation stability and content uniformity for a list of 13 anhydrous suspensions. These results suggest that the anhydrous oral vehicle could serve as a versatile base for pediatric formulation, potentially filling an important gap in pediatric drug delivery. Future studies can further investigate its compatibility, stability and performance with other drugs and in different clinical scenarios.
  • New SuspendIt Anhydrous Base US Pharmacist: A Jobson Publication

Journal Article IconSuspendIt Anhydrous Technical Reports

Journal Article IconVersaBase Journal Articles

  • Case Study: Absorption of Testosterone Cream Via Scrotal Delivery International Journal of Pharmaceutical Compounding
  • Evaluation of the in-vitro Human Skin Percutaneous Absorption of Progesterone in Versabase Using-the Franz Skin Finite Dose Model Journal of Women’s Health Care  pcca logo Abstract
    Abstract: Women may benefit from hormone replacement therapy to alleviate undesirable menopausal symptoms such as hot flashes, disruption of sleep and fatigue. Transdermal hormone replacement therapy consists in the delivery of hormones through the skin and into the blood stream, avoiding gastrointestinal drug absorption difficulties and the first pass effect. Transdermal compounded medications may be customized to meet the individual needs of women by changing the hormones used, the respective concentrations and the medicine’s formulation. Two compounded medications were prepared for progesterone 50 mg/g, as follows: Progesterone in VersaBase® Cream and progesterone in VersaBase® Cream Gel. The purpose of this study is to determine the in vitro human skin percutaneous absorption of progesterone for both test formulations. The Franz Skin Finite Dose Model was the methodology used to evaluate the total absorption, the rate of absorption and the skin content of progesterone applied to the outer surface of ex vivo skin. This model has proven to be a valuable tool for the study of percutaneous absorption of topically applied drugs and to accurately predict in vivo permeation kinetics. The skin samples were obtained within 24 h to 48 h of death from three adult Caucasian donors and a total of 17 Franz diffusion chambers were prepared for testing. Results are presented as the mean ± standard error per parameter, for each test formulation. The rate of percutaneous absorption, presented as mean flux, was similar for the two test formulations and characterized by 2 peaks at approximately 6 hours and 28 hours after dose application, followed by a decline in flux over time. The total absorption and the skin content of progesterone were also similar: 21.6% and 21.8% of the applied doses for the test formulations 1 and 2, respectively. Although in vitro, these results suggest that progesterone in VersaBase® is likely to be delivered through the skin and into the general circulation for systemic effects. Practitioners may then consider transdermal progesterone as a viable route of drug administration for menopausal women.
  • Intravaginal Testosterone Improves Sexual Satisfaction and Vaginal Symptoms Associated With Aromatase Inhibitors The Journal of Clinical Endocrinology and Metabolism
  • Physical and Chemical Stability of Estriol 0.025% to 1% Vaginal Creams (VersaBase) International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Estrogen replacement therapy is often recommended when female patients present with lower than normal physiologic levels, such as patients going through menopause. The physical and chemical stability of estriol 0.25 mg/g and 10 mg/g vaginal creams (VersaBase) was tested over a period of 182 days, at room temperature and refrigerated conditions, in order to determine the corresponding beyond-use date. The physical characterization consisted in observing all samples for color/appearance and odor, and testing for pH, whereas the chemical characterization consisted in ultra-performance liquid chromatography assay testing. Both vaginal creams were proven physically and chemically stable, and the ultra-performance liquid chromatography method was proven stability indicating. As a result, the beyond-use date of the estriol 0.025% to 1% vaginal creams (VersaBase), in electronic mortar and pestle plastic jars, is six months at both room temperature and refrigerated conditions.
  • Pilot Study: Absorption and Efficacy of Multiple Hormones Delivered in a Single Cream Applied to the Mucous Membranes of the Labia and Vagina Gynecologic and Obstetric Investigation
  • Progesterone 50 mg/g in VersaBase Cream US Pharmacist: A Jobson Publication

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PCCA PostersVersaBase Scientific Posters

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Journal Article IconVersaBase Anhydrous HRT Case Studies

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Journal Article IconVersaBase Anhydrous HRT Journal Articles

  • Evaluation of an Anhydrous Permeation-Enhancing Vehicle for Percutaneous Absorption of Hormones AAPS PharmSciTech pcca logo Abstract
    Abstract: The efficiency and safety of hormone delivery through the skin partly depend on the appropriate choice of vehicle and the type of formulation. The present study reports the skin cytotoxicity, irritancy, and safety of a newly developed anhydrous permeation-enhancing base (APEB) and the percutaneous absorption of progesterone, testosterone, estriol, and estradiol in APEB formulations. Using the human skin EpiDerm model, cell death was not observed after 4 h of exposure to APEB and was 48% after 24 h, indicating its mild to non-irritating property. APEB did not change the expression level of skin cell proliferation markers including PCNA, MCL-1, iNOS, and NFκB proteins, and apoptosis was minimal after 8-h exposure. The in vivo skin irritation and sensitization evaluation of APEB using a Human Repeat Insult Patch Test showed no adverse reaction of any kind during the course of the study. These results indicate the safety of APEB on skin tissues. The hormone percutaneous absorption was performed using human cadaver abdomen skin tissues and the Franz diffusion system, and hormone concentrations were determined by ELISA. Absorption was observed as early as 2 h of application and accumulated after 24 h to 2851 ± 66 ng/cm2, 2338 ± 594 ng/cm2, 55 ± 25 ng/cm2, and 341 ± 122 ng/cm2 for progesterone, testosterone, estriol, and estradiol, respectively. A steady flux rate of absorption of the hormones was observed within 24 h of application. These results suggest that APEB can be used as a vehicle to deliver these hormones through the skin and into the bloodstream for hormone replacement therapy.
  • In vitro Evaluation of the Percutaneous Absorption of Progesterone in Anhydrous Permeation-Enhancing Base Using the Franz Skin Finite Dose Model and Mass Spectrometry Archives of Dermatological Research pcca logo Abstract
    Abstract: Progesterone is used for hormone replacement therapy through various routes of administration. This study was conducted to (a) evaluate the stability of progesterone in a proprietary anhydrous permeation-enhancing base (APEB) and the efficiency of its skin permeation, and (b) determine the appropriateness of mass spectrometry as a method of analysis for permeated progesterone. Using a proven stability-indicating ultra-performance liquid chromatographic method, the compounded hormone (100 mg progesterone/g APEB gel) was determined to be physically and chemically stable at room temperature for six months. Skin permeation analysis using the Franz skin finite dose model and mass spectrometry imaging showed an optical density of 1699 for the permeated progesterone compounded in APEB and 550 for the permeated progesterone in a water containing VBC, which is a statistically significant different (P = 0.029). The study suggests that APEB can be used as a compounding base for effective skin permeation of progesterone, and mass spectrometry is a reliable method for visualization and quantitative analysis of permeated progesterone.

Journal Article IconVersaBase Anhydrous HRT Scientific Posters

Journal Article IconVersaBase Anhydrous HRT Technical Reports

Journal Article IconXemaTop Journal Articles

  • Evaluation of the Efficacy and Stability of Compounded Pentoxifylline-Containing XemaTop™ for Psoriasis International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Psoriasis is an inflammation-mediated skin disorder for which an efficacious topical treatment is yet to be identified. A new compounded topical formulation containing 10% pentoxifylline in XemaTop base was recently developed for psoriasis. Prior to its use in humans, an in vitro evaluation was performed to determine its efficacy in attenuating molecular markers associated with psoriasis using a three-dimensional psoriasis tissue model. After 5 days of topical exposure to the formulation, the levels of inflammatory cytokines IL-1ß, IL-6, and GM-CSF decreased by 20%, 94%, and 96%, respectively. The production of pro-collagen type I and fibronectin essential for cellular proliferation was also significantly inhibited with a concomitant thinning of the epidermis. These results suggest that 10% pentoxifylline in XemaTop is efficacious in inhibiting the biomarkers associated with psoriasis. Pentoxifylline in XemaTop was stable within 91 days when stored under refrigerated or ambient conditions. These biochemical and stability studies suggest that 10% pentoxifylline in XemaTop may be evaluated now in psoriasis patients.
  • In Vitro Evaluation of Naltrexone HCl 1% Topical Cream in XemaTop™ for Psoriasis Archives of Dermatological Research pcca logo Abstract
    Abstract: Psoriasis is a multifactorial skin disease involving abnormal cell proliferation and inflammation; an efficacious topical treatment is yet to be identified. A formulation containing 1% Naltrexone HCl in XemaTop™ base was compounded, characterized and evaluated in vitro as a possible treatment for psoriasis. A three-dimensional psoriasis tissue model was exposed to the formulation for 2 or 5 days and analyzed for the level of markers of cellular proliferation, and inflammatory cytokine IL-6. Using immunohistochemical staining, the level of Ki67 protein significantly decreased in the drug-treated tissues. Western blot analysis showed 86% and 53% down-regulation of other proliferation markers PCNA and CYCLIN D1, respectively, after 5-day exposure. The pro-survival Wnt/β-catenin pathway was compromised as indicated by 57% decrease in the level of β-CATENIN and down-regulation of its down-stream targets including CYCLIN D1 (decreased by 53%), c-MYC (63%), c-JUN (92%) and MET (96%) proteins. Likewise, the PI3K/AKT/mTOR pathway was significantly inhibited by 1% Naltrexone HCl in XemaTop™, suggesting protein synthesis was affected. The production of IL-6 was inhibited by 70% in drug-treated tissues. These results suggest that the compounded drug is efficacious in down-regulating molecular markers associated with the pathogenesis of psoriasis. Low-dose Naltrexone in XemaTop™ was stable within 180 days when stored under refrigerated or ambient conditions. These results provide a basis for a clinical evaluation of 1% Naltrexone HCl in XemaTop™ in psoriasis patients.
  • Management of Psoriasis with a XemaTop Topical Compounded Formula: A Case Report  International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Skin conditions such as psoriasis and eczema negatively impact the patient’s quality of life; the primary goal of topical treatments is to minimize the disease-specific symptoms. This case report discusses the management of two refractory psoriasis skin lesions in an adult male using a topical compounded formula. The psoriasis symptoms were assessed quantitatively using two validated research instruments, the Psoriasis Symptom Inventory, and an adapted Numeric Rating Scale. A qualitative assessment was also performed by evaluating the digital photographs taken by the patient during the course of treatment. The compounded formula containing zinc pyrithione, clobetasol propionate, and cyanocobalamin in the Professional Compounding Centers of America’s proprietary base PCCA XemaTop, applied topically for three weeks, significantly reduced the patient’s self-reported psoriasis symptoms and improved his overall condition by 81.2%. This successful case report is important evidence for healthcare professionals when considering new, innovative topical compounded formulas for managing skin conditions such as psoriasis and eczema.

Journal Article IconXemaTop Technical Reports

Journal Article IconXemaTop Case Studies

  • Hand-Foot Syndrome Induced by Chemotherapy
  • Management of Psoriasis with a XemaTop Topical Compounded Formula: A Case Report  International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Skin conditions such as psoriasis and eczema negatively impact the patient’s quality of life; the primary goal of topical treatments is to minimize the disease-specific symptoms. This case report discusses the management of two refractory psoriasis skin lesions in an adult male using a topical compounded formula. The psoriasis symptoms were assessed quantitatively using two validated research instruments, the Psoriasis Symptom Inventory, and an adapted Numeric Rating Scale. A qualitative assessment was also performed by evaluating the digital photographs taken by the patient during the course of treatment. The compounded formula containing zinc pyrithione, clobetasol propionate, and cyanocobalamin in the Professional Compounding Centers of America’s proprietary base PCCA XemaTop, applied topically for three weeks, significantly reduced the patient’s self-reported psoriasis symptoms and improved his overall condition by 81.2%. This successful case report is important evidence for healthcare professionals when considering new, innovative topical compounded formulas for managing skin conditions such as psoriasis and eczema.

PCCA PostersXemaTop Scientific Posters

Journal Article Icon XemaTop USP Monographs

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Pediatric

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Journal Article IconActive Ingredients

  • Beyond-use Date of Trimix: A Reproducible Stability Study Using Bracketing Design International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Trimix is a widely prescribed penile injection for patients with erectile dysfunction and is only available as a compounded medication. The instability of alprostadil, one of the major ingredients of Trimix, has been a limiting factor in its utilization. There are published stability data for Trimix formulations that have been used to establish a beyond-use-date. However, a robust bracketed study that is shown to be reproducible is highly desirable and meaningful. The purpose of this study was to test the reproducibility of a bracketed stability study when the preparations were made by two different entities to provide beyond-use date information of Trimix preparations that cover a wide range of strengths. A validated stability indicating method was used to compare the stability of a bracketed Trimix - alprostadil 5 µg/mL to 45 µg/mL, papaverine 15 mg/mL to 30 mg/mL, and phentolamine 0.4 mg/mL to 5 mg/mL, and a single-strength preparation containing alprostadil 30 µg/mL, papaverine 30 mg/mL, and phentolamine 2 mg/mL that were compounded and stored following the same methods and conditions, but at two different practice settings. Beyond-use dates of 60 days and 64 days at cold temperature were obtained for the two preparations from two different settings. The consistent results confirmed the reproducibility of the bracketing designs used to determine the beyond-use dates of Trimix. The clinical value of these results stems from the availability of accurate and widely applicable stability data that can be referenced to establish beyond use dates of a number of Trimix preparations with various strength combinations.
  • Clinical Efficacy of a Topical Compounded Formulation in Male Androgenetic Alopecia: Minoxidil 10%, Finasteride 0.1%, Biotin 0.2%, and Caffeine Citrate 0.05% Hydroalcoholic Solution  International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Androgenetic alopecia is the most common form of hair loss. This condition affects both men and women causing significant psychological distress and a decrease in the quality of life. The objective of this study was to investigate the clinical efficacy and patient satisfaction of a topical compounded formulation (minoxidil 10%, finasteride 0.1%, biotin 0.2%, and caffeine citrate 0.05% hydroalcoholic solution) in male androgenetic alopecia patients. A total of five individual, prospective case studies were conducted in the private hair transplant practice of Dr. James C. Marotta. Patients were provided with the topical formulation and instructed to apply a measured 1-mL dose to the entire frontal, parietal, and occipital scalp, twice daily for 6 months. Patients visited the practice periodically (90 days, 120 days, and 180 days post-treatment) for clinical evaluation, photographic assessment, and measurement of their treatment satisfaction by the Men’s Hair Growth Questionnaire. By the end of the study, at 180 days, the dermatologist-in-charge concluded that the topical treatment was successful for all five patients. Although moderate, the clinical improvements were visually noticeable as most patients had thicker, more voluminous hair; improved scalp coverage; and improved general hair appearance. These results were consistent with the photographic assessment, which demonstrated a global average increase of +1.05 in the patients’ hair density. According to the patients’ self-assessment, the topical compounded formulation was effective following 3 months and 6 months of continuous treatment. At 120 days, the patients’ satisfaction was neutral or negative, which was likely due to negligible differences in the patients’ hair growth and appearance in 90 days compared to 120 days. The results from this study suggest that the new hair-loss topical solution may be considered a safe and effective treatment option in male AGA patients.
  • Physicochemical Stability of Extemporaneously Prepared Methylcobalamin Injections in the Presence and Absence of Preservative and the Impact of Light Exposure International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Methylcobalamin, one of the two active forms of vitamin B12, is the most effective analog in permeation and in transportation of neurons in subcellular organelles. Formulations of methylcobalamin are only commercially available in a few countries, which make them inaccessible for most patients. Extemporaneously prepared injections become the only option for those patients. The objective of this work is to study the physical and chemical (ultrahigh- performance liquid chromatography stability-indicating method) stabilities of methylcobalamin injections in the presence and absence of preservative during 181 days (considering the stability limit as 90% of initial concentration of methylcobalamin). The light exposure stability of injections in amber serum vials or clear syringes, solution in amber or clear glassware under typical pharmacy, clinical, and laboratory settings are also presented. Methylcobalamin injections, regardless of the concentrations and inactive ingredients, remained stable for at least 181 days at room temperature when stored in amber serum vials and protected from light. These experimental data suggested that the methylcobalamin injection solutions should be protected from light completely and light exposure in pharmacy, clinical, and laboratory setting should be minimized.
  • The Potential Effects of a Compounded Methylcobalamin Nasal Spray on Short-term Memory Loss after Intracranial Hemorrhage: A Case Report International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Short-term memory loss is a common complication after intracranial hemorrhage or traumatic brain injury. FDA-approved cholinesterase inhibitors for memory symptoms of Alzheimer’s disease have not been proven effective for improving memory impairment resulting from a hemorrhagic event. The purpose of this case study was to present the potential effectiveness of a compounded nasal spray containing methylcobalamin in improving short-term memory function in a patient post-intracranial hemorrhage. The patient started to administer the methylcobalamin nasal spray once daily after suffering from short-term memory loss for four years. His verbal memory, visual memory, and quality of life were assessed by the Hopkins Verbal Learning Test–Revised, Benton Visual Retention Test, and the 36-Item Short Form Survey, respectively, at baseline and 30 days after treatment. The delayed recall test was repeated after 60 days. After 30 days of treatment, the patient received improved scores in both verbal and visual memory tests, as well as improved self-reported quality of life. The patient became less dependent on phone reminders in daily life. The improvement in delayed recall remained significant after 60 days of treatment. This case report suggests a potentially safe and effective therapy for attenuating short-term memory impairment after intracranial hemorrhage.

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Journal Article IconcBHT

  • P6. Compounded Hormones for Female Patients: A Survey Assessment of Clinical Practices in the United States
  • Compounded Hormones for Female Patients: A Survey Assessment of Clinical Practices in the U.S.  (NAMS) 2021 Annual Meeting
  • Safety and Efficacy of Compounded Bioidentical Hormone Therapy (cBHT) in Perimenopausal and Postmenopausal Women a Systematic Review and Meta-Analysis of Randomized Controlled Trials Menopause: The Journal of The North American Menopause Society pcca logo Abstract
    Importance: More information is needed about the efficacy and safety of compounded bioidentical hormone therapy (cBHT) in the published literature. A thorough synthesis of existing data is not currently available.

    Objective: To provide a systematic review and meta-analysis of the existing evidence related to the safety and efficacy of commonly prescribed cBHT preparations in perimenopausal and postmenopausal women.

    Evidence Review: PubMed, ClinicalTrials.gov, and The Cochrane Central Register of Controlled Trials were searched. Randomized controlled trials (RCTs) comparing cBHT with a placebo or FDA-approved products in perimenopausal or postmenopausal women were eligible. The risk of bias was assessed by the Cochrane risk of bias tool. The primary safety outcome was changes in lipid profile and glucose metabolism, and the primary efficacy outcome was the change of vaginal atrophy symptoms. The secondary outcomes included the change of endometrial thickness, risk of adverse events, vasomotor symptoms, change of serum hormone levels, and change of bone mineral density.

    Findings: A total of 29 RCTs reported in 40 articles containing 1,808 perimenopausal and postmenopausal women were included. Two risk factors of cardiovascular disease, lipid profile, and glucose metabolism, were evaluated with cBHT. The results showed that compounded androgen was not associated with change of lipid profile or glucose metabolism. There was no change in endometrial thickness or serious adverse events. There were more androgenic side effects with compounded dehydroepiandrosterone compared with placebo as expected. Other safety measures including clinical cardiovascular events, endometrial biopsy, and risk of breast cancer were not studied. cBHT in the form of compounded vaginal androgen was found to significantly improve vaginal atrophy symptoms (SMD -0.66 [95% CI, -1.28 to -0.04]; I2 = 86.70%). This finding was supported by the association between compounded vaginal androgen and improved female sexual function scores. The changes of serum hormone levels were also evaluated. Despite the variations in absorption from different types of compounded hormones, routes, and strengths, the trends were consistent with published data from FDA-approved products.

    Conclusions and Relevance: This review found that cBHT used in primarily short-term RCTs is not associated with adverse changes in lipid profile or glucose metabolism. cBHT in the form of vaginal androgens appears beneficial for vaginal atrophy symptoms. There are insufficient RCTs of cBHT to assess clinical risk of breast cancer, endometrial cancer, or cardiovascular disease. Long-term studies with clinical endpoints are needed.

    In 2002, the Women’s Health Initiative reported the health risks of oral conjugated equine estrogen with medroxyprogesterone acetate in postmenopausal women.1 Since then, a substantial group of postmenopausal women using hormone therapy (HT) made the decision with their treating physicians to switch from synthetic hormones to bioidentical hormone therapy. Some physicians and patients determined that compounded bioidentical hormone therapy (cBHT) was appropriate. Several nationwide surveys showed a significant decline in prescriptions of FDA-approved hormone products over the past decade, in contrast with a continuous growth in cBHT. It was estimated that 1 to 2.5 million US women are cBHT users, and 26 to 33 million cBHT prescriptions were filled each year.2-4 The new trend in HT raised concerns and discussions surrounding cBHT. The most prominent advantages of cBHT are its personalized approach and the flexibility in making customized strengths and dosage forms. Black box warnings are required on all FDA-approved estradiol and topical testosterone products, and Federal law exempts all compounded drugs from such labeling requirements. However, besides the absence of boxed warnings, other safety considerations regarding cBHT arose among physicians. These safety concerns included the increased risk of endometrial cancer, inconsistency of drug content, incomplete adverse events reporting, and unknown risk of cardiovascular disease, mostly from survey findings, case reports, nonrandomized studies, and expert opinions.5,6 Because of concerns regarding cBHT, in 2018, the FDA requested the National Academies of Science, Engineering, and Medicine (NASEM) to evaluate the available evidence of cBHT regarding safety and effectiveness.5 Thirteen clinical trials with relevance to the safety and effectiveness of cBHT were highlighted and discussed by the NASEM committee. A conclusion was reached that there was a lack of high-quality research to establish the safety and effectiveness of cBHT.5 Furthermore, the highest level of evidence, a systematic review and meta-analysis had not been published. mucu

    We conducted a deep and thorough literature search and identified some studies that have not been cited by others in this field, including the NASEM committee. To obtain a comprehensive view of the safety and efficacy of commonly prescribed cBHT preparations, and to evaluate the robustness of evidence for using cBHT, we performed a systematic review and meta-analysis of randomized controlled trials (RCTs) to examine the safety and efficacy of cBHT in perimenopausal and postmenopausal women. In this review, the analyzed safety outcomes included two risk factors of cardiovascular disease, endometrial thickness, and adverse events. There were no available data on other measures of safety such as breast density on mammography, breast cancer, or clinical cardiovascular events. The primary efficacy outcome is vaginal atrophy symptoms. Change of serum hormone levels were also evaluated as a secondary outcome to provide information on absorption.

Journal Article IconClarifying Base

  • Combination Therapy of Oral LDN and Topical Pentoxifylline, Rifampin, Clindamycin for Hidradenitis Suppurativa International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Hidradenitis Suppurativa (HS) is a chronic inflammatory skin disease that may have profound effects on the patient’s quality of life. A personalized HS combination therapy treatment was prescribed to a 54-year-old female suffering from multiple painful sores, as follows: naltrexone capsules titrated from 0.5 mg up to 4.5 mg; pentoxifylline 5%, rifampin 2%, clindamycin 1%, and glycolic acid topical cream. Clinical improvements were observed using two disease-specific outcome measures: Hurley Staging System and HS Score. The patient’s HS improved from Stage II (moderate) to Stage I (mild), and the HS score decreased from 103 points with five anatomical regions reported, to 19 points with only three regions affected. Furthermore, the before and after treatment photographs showed a visible reduction in the number of boils/skin abscesses and an overall recovery. Improvements were also observed across all domains of the patient’s self-reported quality of life (Hidradenitis Suppurativa Quality of Life Assessment). The patient did not experience any undesirable effects. Compounded medications may be customized to meet the patient’s special needs and may be adjusted throughout the course of treatment to match the patient’s individual progress. Although further studies are necessary, this personalized, combination therapy may be a key treatment option in HS.

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Case Study IconNataTroche

Case Study IconPoloxamer Gel

Journal Article IconPermE8 Anhydrous Gel

  • Evaluation of the in vitro Human Skin Percutaneous Absorption of Ketoprofen in PCCA PermE8™ Anhydrous Gel vs. PCCA Lipoderm®
  • Evaluation of the in vitro Human Skin Percutaneous Absorption of Ketoprofen in Topical Anhydrous and Aqueous Gels Skin Research & Technology pcca logo Abstract
    Background: Ketoprofen is a nonsteroidal anti-inflammatory drug used for the treatment of acute and chronic pain associated with inflammatory conditions. This study aims to evaluate the in vitro percutaneous absorption of ketoprofen 10% formulated in proprietary anhydrous and aqueous gels using the Franz skin finite dose model.
    Materials and Methods: The anhydrous gel was initially characterized for cytotoxicity using EpiDerm skin tissue model by cell proliferation assay and Western blot analysis. The Ultra Performance Liquid Chromatography method for measuring ketoprofen was validated and the stability of ketoprofen 10% in the anhydrous gel formulation was evaluated at 5°C and 25°C for 181 days. The percutaneous absorption of ketoprofen was determined using donated human skin. The tissue sections were mounted within Franz diffusion cells. A variable finite dose of each ketoprofen formulation in either anhydrous or aqueous gel was applied to the skin sections and receptor solutions were collected at various time points.
    Results: Cell proliferation assay showed minimal cell death when EpiDerm skin tissue was exposed to the anhydrous gel for 24 h; the levels of protein markers of cell proliferation were not affected after 17-h exposure. Ketoprofen was stable in the anhydrous gel when stored at 5°C and 25°C. When compounded in the anhydrous and aqueous gels, ketoprofen had mean flux rate of 2.22 and 2.50 μg/cm2/h, respectively, after 48 h. The drug was distributed to the epidermis and dermis sections of the skin. Both the anhydrous and aqueous gels facilitated the percutaneous absorption of ketoprofen without statistically significant differences.
    Conclusion: The anhydrous gel can be used as a base to facilitate the transdermal delivery of ketoprofen. Although the anhydrous and aqueous gels can deliver a similar amount of ketoprofen, the anhydrous gel (water activity below 0.6) allows for extended default beyond-use-date of compounding preparations.
  • Evaluation of Safety and Skin Irritancy of PermE8 Anhydrous Gel in Human Epidermis Model

Case Study IconPolyox Bandage

Case Study IconRapid Dissolve Tablet Powder

Case Study IconSorbitol Lollipop

  • Glycopyrrolate Sorbitol Lollipops for Drooling: Two Case Reports International Journal of Pharmaceutical Compounding pcca logo Abstract
    Abstract: Drooling is a pathologic condition that is commonly associated with neurodisability and poor quality of life. An elderly dementia patient and an adult cancer patient suffered from persistent drooling, and they were both prescribed glycopyrrolate 0.5-mg sorbitol lollipops, per recommendation of their local compounding pharmacist. The severity and frequency of drooling decreased substantially in both patients, and there were no reported adverse effects. These two case reports demonstrate the safety and efficacy of glycopyrrolate lollipops in managing excessive salivation, as well as the importance of the triad relationship in addressing the individual patient needs.

Journal Article IconSpira-Wash

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Journal Article IconW06 Anhydrous Topical Gel

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Journal Article IconZosil